Wednesday, April 10, 2019

Molar Mass by Free

Molar Mass by Freezing Point Depression EssayProceduresWeigh the taste organ pipe. Assemble the apparatus of thermometer, split stopper, and stirrer. Measure about eight grams of BHT into the runnel organ pipe. Record the combined chaw, and the mass of the BHT. Clamp the establish tube in the beaker and insert the thermometer and rousing wire assembly into the test tube and clamp the assembly to the ring stand. The thermometer should on top of the solid. Add water to the beaker so that the solid is comfortably below the level of the water. Heat the water bath to about 90 Celsius. Allow the BHT in the test tube to melt. When the temperature of the BHT is 80 Celsius or higher, remove the thermometer and test tube from the water bath.The thermometer should maintain position in proportion to the BHT, but the test tube should be out of the water bath beaker. Record the temperature of the BHT either 20 seconds for 30 minutes. Stir the BHT until it solidifies. Measure and rec ord approximately one gram of cetyl alcoholic drink. Place the cetyl alcohol in the test tube containing the BHT. Replace the test tube to the water bath. Heat the test tube until the unions are melted, and reach a temperature over 80 Celsius. Once it exceeds 80 C, remove the test tube from the water bath but maintain the thermometer position in proportion to the mixture. Record the temperature of the BHT every 20 seconds for 30 minutes. Stir the mixture until it solidifies. Repeat the above steps with fresh BHT and, a clean test tube, thermometer, stirrer, and approximately one gram of the unknown compound in place of the cetyl alcohol.AnalysisFor the lab, the calculated percentage error was 2.99%. The percent error came from the difference in the grinder mass of the unknown substance as experienced in the lab, and in the accepted entropy. A possible point of error was in whether or not a group stirred the substance as it was cooling. This would affect the selective informatio n recorded, and skew the results depending on how constant the stirring was between trials. If the lab were to be preformed again, the students would all have the same amount of stirring of the cooling substance, either none at all, or a constant stirring throughout the 30 minute cooling period.ConclusionThe purpose of this lab was to determine the molar mass of an unknown substance by measuring the freezing point depression of a solution of an unknown substance and BHT, and to comparison the data collected with the accepted value for the lab. The purpose of the lab was fulfilled as the students determined the molar mass of the unknown substance, despite much struggle throughout the process of the lab. Much of the class data was extremely off of the range of acceptable margin of error, so all groups are using the data from a successful group to perform the report.

No comments:

Post a Comment

Note: Only a member of this blog may post a comment.